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毕业论文网 > 任务书 > 化学化工与生命科学类 > 应用化学 > 正文

氮杂环丙烯化合物的合成新方法任务书

 2020-05-24 12:34:04  

1. 毕业设计(论文)的内容和要求

1.熟悉基本的实验操作,理解实验的基本内容;2.能做做到流利阅读文献,掌握文献内容;3.熟练运用各种信息平台查阅相关信息;4.了解当下有机化学方向中氮杂三元环的内容,了解氮杂三元环的背景以及意义;5.熟悉并掌握氮杂三元环合成的机理。

2. 参考文献

[1]Presset Marc,Coquerel Yoann,Rodriguez Jean. Microwave-assisted Wolff rearrangement of cyclic 2-diazo-1,3-diketones: an eco-compatible route to alpha-carbonylated cycloalkanones. The Journal of Organic Chemistry,2008,741:. [2]Fontaine Patrice,Masson G#233;raldine,Zhu Jieping. Synthesis of pyrroles by consecutive multicomponent reaction/[4 1] cycloaddition of alpha-iminonitriles with isocyanides. Organic Letters,2009,117:. [3]Fan Hui,Peng Jiangnan,Hamann Mark T,Hu Jin-Feng. Lamellarins and related pyrrole-derived alkaloids from marine organisms. Chemical Reviews,2007,1081:. [4]Skepper Colin K,Molinski Tadeusz F. Long-chain 2H-azirines with heterogeneous terminal halogenation from the marine sponge Dysidea fragilis. The Journal of Organic Chemistry,2008,737:. [5]de Lucas N C,Netto-Ferreira J C,Andraos J,Scaiano J C. Nucleophilicity toward ketenes: rate constants for addition of amines to aryl ketenes in acetonitrile solution.[J]. The Journal of Organic Chemistry,2001,6615:. [6]Bharadwaj Ashwin R,Scheidt Karl A. Catalytic multicomponent synthesis of highly substituted pyrroles utilizing a one-pot sila-Stetter/Paal-Knorr strategy.[J]. Organic Letters,2004,614:. [7]Fujita Masaki,Nakao Yoichi,Matsunaga Shigeki,Seiki Motoharu,Itoh Yoshifumi,Yamashita Jun,Van Soest Rob W M,Fusetani Nobuhiro. Ageladine A: an antiangiogenic matrixmetalloproteinase inhibitor from the marine sponge Agelas nakamurai. American Chemical Society. Journal,2003,12551:. [8]Alois F#252;rstner. Chemistry and Biology of Roseophilin and the Prodigiosin Alkaloids: A Survey of the Last 2500 Years. Angewandte Chemie International Edition,2003,4231:. [9]Padwa A,Eisenberg W. Photochemical transformations of small ring carbonyl compounds. XXXIX. Photochemical synthesis and chemical reactivity of the tricyclo(3.2.0.0 2,6 )heptan-7-ol system. American Chemical Society. Journal,1972,9416:. [10]St Cyr Daniel J,Arndtsen Bruce A. A new use of Wittig-type reagents as 1,3-dipolar cycloaddition precursors and in pyrrole synthesis. American Chemical Society. Journal,2007,12941:.

3. 毕业设计(论文)进程安排

毕业设计进程安排: 2016.3.1 进入实验室,交待相关事宜,安排实验任务; 2016.3.1-2016.3.4 查阅文献,准备开题报告; 2016.3.10 提交开题报告。

2016.3.10-2015.3.31合理设计实验,进行实验操作。

2016.4.1-2015.5.29筛选条件,优化反应条件;2015.5.30-2015.6.4 实验数据整理与分析。

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