钛酸钾晶须的溶液纺丝及其在尼龙复合中的应用任务书
2020-04-25 20:20:39
1. 毕业设计(论文)的内容和要求
内容: 1.查阅文献,掌握水热法制备钛酸钾晶须方法及基本原理 2.熟悉溶液纺丝技术实验 3.熟悉SEM以及XRD等测试仪器的操作技能 要求: 1探究晶须材料的不同分层剥离条件 2.不同种类的晶须,及其剥离材料与尼龙复合的效果 3.整理实验数据,得出优化的复合条件
2. 参考文献
[1]. Masaki, N. and S. Uchida, et al. (2002). "Characterization of a New Potassium Titanate, KTiO2(OH) Synthesized via Hydrothermal Method." Chemistry of Materials 14 (1): 419-424. [2]. Meng, X. and D. Wang, et al. (2006). "Effects of titania different phases on the microstructure and properties of K2Ti6O13 nanowires." Solid State Communications 137 (3): 146-149. [3]. Tomiha, M. and N. Masaki, et al. (2002). "Hydrothermal synthesis of alkali titanates from nano size titania powder." Journal of Materials Science 37 (11): 2341-2344. [4]. Yahya, R. B. and H. Hayashi, et al. (2001). "Hydrothermal Synthesis of Potassium Hexatitanates under Subcritical and Supercritical Water Conditions and Its Application in Photocatalysis." Chemistry of Materials 13 (3): 842-847. [5]. Masaki, N. and S. Uchida, et al. (2000). "Hydrothermal synthesis of potassium titanates in Ti-KOH-H2O system." Journal of Materials Science 35 (13): 3307-3311. [6]. Sikhwivhilu, L. M. and S. Sinha Ray, et al. (2009). "Influence of bases on hydrothermal synthesis of titanate nanostructures." Applied Physics A: Materials Science Processing 94 (4): 963-973. [7]. Bavykin, D. V. and B. A. Cressey, et al. (2007). "Low-temperature synthesis of titanate nanotubes in aqueous KOH." Australian Journal of Chemistry 60 (2): 95-98. [8]. Zhang, J. and Y. Wang, et al. (2006). "Microwave-assisted synthesis of potassium titanate nanowires." Materials Letters 60 (24): 3015-3017. [9]. Du, G. H. and Q. Chen, et al. (2003). "Potassium titanate nanowires: Structure, growth, and optical properties." Physical Review B: Condensed Matter and Materials Physics 67 (3): 035323/1-035323/7. [10]. Oota, T. and H. Saito, et al. (1979). "Synthesis of potassium hexatitanate fibers by the hydrothermal dehydration method." Journal of Crystal Growth 46 (3): 331-8. [11]. Shimizu, O. and Y. Muramatsu, et al. (1986). "Characteristics of optical fibers jacketed with a thermoplastic resin filled with potassium titanate whiskers." Proceedings of International Wire and Cable Symposium 35th: 166-73. [12]. Yang, B. and M. Zhang, et al. (2017). "Effects of potassium titanate whiskers on the mechanical and thermal properties of poly (para-phenylene terephthalamide) paper sheet." Polymer Composites 38 (7): 1390-1395. [13]. Lu, J. and X. Lu (2001). "Elastic interlayer toughening of potassium titanate whiskers-nylon 66 composites and their fractal research." Journal of Applied Polymer Science 82 (2): 368-374. [14]. Satomi, E. and M. Chatani, et al. (1980). "Filler effects of potassium titanate fibers on injection molding characteristics and mechanical properties of thermoplastic resins." Osaka-furitsu Kogyo Gijutsu Kenkyusho Hokoku(77): 49-54. [15]. Lu, J. and Q. Dou, et al. (2001). "Fractal research of fracture surfaces of potassium titanate whiskers toughened nylon 66." Gaofenzi Cailiao Kexue Yu Gongcheng 17 (2): 154-157. [16]. Yuchun, O. and Y. Feng, et al. (1997). "Interfacial interaction and mechanical properties of Nylon 6-potassium titanate composites prepared by in-situ polymerization." Journal of Applied Polymer Science 64 (12): 2317-2322. [17]. Lu, J. and F. Xin, et al. (2001). "Mechanical properties of potassium titanate whisker-rubber-nylon 66 composites." Nanjing Huagong Daxue Xuebao, Ziran Kexueban 23 (1): 6-9. [18]. Li, C. and W. Mu, et al. (2008). "Moisture absorbing ability and tribology capability of potassium titanate whiskers reinforced MC nylon." Fuhe Cailiao Xuebao 25 (5): 69-73.
3. 毕业设计(论文)进程安排
进度安排 2019年 2月22日-3月09日 根据课题要求,查阅文献; 3月10日-3月14日 翻译外文文献; 3月15日-3月25日 撰写开题报告; 3月26日-5月15日 用各种表征仪器测取各种数据; 5月 16日- 数据处理;撰写论文;论文预答辩、答辩。
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