新型二维材料g-C3N4的剥离及气体分离膜的制备任务书
2020-04-21 17:13:22
1. 毕业设计(论文)的内容和要求
研究内容: (1)探究高质量块状C3N4前驱体的烧结条件; (2)考察热腐蚀法中的腐蚀时间对C3N4形貌的影响; (3)探究超声剥离C3N4纳米片的最优参数; (4)制备C3N4气体分离膜并测试性能。
具体要求: (1)大量阅读文献(英文文献20篇以上,中文文献10篇以上); (2)熟悉实验室基本仪器的操作; (3)掌握测试表征的基本原理、操作方法; (4)学会膜性能的测试方法; (5)具备独立撰写论文、制作学术PPT并汇报课题的能力。
2. 参考文献
[1] Ma T Y, Tang Y, Dai S, et al. Proton-Functionalized Two-Dimensional Graphitic Carbon Nitride Nanosheet: An Excellent Metal-/Label-Free Biosensing Platform [J]. Small, 2014, 10(12): 2382-2389 [2] Niu P, Zhang L, Liu G, et al. Graphene-Like Carbon Nitride Nanosheets for Improved Photocatalytic Activities [J]. Advanced Functional Materials, 2012, 22(22): 4763-4770 [3] Schwinghammer K, Mesch M B, Duppel V, et al. Crystalline Carbon Nitride Nanosheets for Improved Visible-Light Hydrogen Evolution [J]. Journal Of the American Chemical Society, 2014, 136(5): 1730-1733 [4] Wang Y, Li L, Wei Y, et al. Water Transport with Ultralow Friction through Partially Exfoliated g-C3N4 Nanosheet Membranes with Self-Supporting Spacers [J]. Angewandte Chemie-International Edition, 2017, 56(31): 8974-8980 [5] Xu J, Zhang L, Shi R, et al. Chemical exfoliation of graphitic carbon nitride for efficient heterogeneous photocatalysis [J]. Journal Of Materials Chemistry A, 2013, 1(46): 14766-14772 [6] Yang S, Gong Y, Zhang J, et al. Exfoliated Graphitic Carbon Nitride Nanosheets as Efficient Catalysts for Hydrogen Evolution Under Visible Light [J]. Advanced Materials, 2013, 25(17): 2452-2456 [7] Yin Y, Han J, Zhang X, et al. Facile synthesis of few-layer-thick carbon nitride nanosheets by liquid ammonia-assisted lithiation method and their photocatalytic redox properties [J]. Rsc Advances, 2014, 4(62): 32690-32697 [8] Zhang J, Chen Y, Wang X. Two-dimensional covalent carbon nitride nanosheets: synthesis, functionalization, and applications [J]. Energy Environmental Science, 2015, 8(11): 3092-3108 [9] Zhang X, Xie X, Wang H, et al. Enhanced Photoresponsive Ultrathin Graphitic-Phase C3N4 Nanosheets for Bioimaging [J]. Journal Of the American Chemical Society, 2013, 135(1): 18-21 [10] Zhou K-G, McManus D, Prestat E, et al. Self-catalytic membrane photo-reactor made of carbon nitride nanosheets [J]. Journal Of Materials Chemistry A, 2016, 4(30): 11666-11671
3. 毕业设计(论文)进程安排
19.2.15~19.3.10 查阅文献,开题报告,掌握基础实验技能 19.3.10~19.5.1 确定实验方案,正式开展实验工作 19.5.1~19.5.28 中后期实验阶段及数据收集 19.5.28~19.6.15 数据整理,撰写论文,准备答辩
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