1. 毕业设计（论文）的内容和要求

本实验的研究内容为利用油酸甲酯中的双键，通过硅氢加成反应接枝聚硅氧烷，制备出烷基改性硅油，提高润滑性能。

2. 参考文献

[1] M. Mazurek, D.J. Kinning, T. Kinoshita, Novel material based on silicone-acrylate copolymer networks, J. Appl. Polym. Sci. 80 (2) (2001) 159-180. [2] G.O. Yahaya, B.J. Brisdon, M. Maxwell, R. England, Preparation and properties of functionalized polyorganosiloxanes, J. Appl. Polym. Sci. 82 (4) (2001) 808-817. [3] Y. Xuefeng, Y. Cheng, Synthesis and comparative properties of poly(dimethylsiloxane) grafted alkyl acrylate, J. Appl. Polym. Sci. 106 (6) (2007) 3600-3604. [4] K. Xie, A. Hou, Y. Shi, J. Yu, The surface polymerising of fluoromonomerand the shade-darkening effect on dyed polyester microfibre fabric, Color. Technol. 123 (5) (2007) 293-297. [5] W.M. Raslan, A. Bendak, Changes induced in silk-like polyester properties by alkoxides treatment, J. Appl. Polym. Sci. 98 (4) (2005) 1829-1837. [6] K. Xie, A. Hou, Y. Shi, Synthesis of fluorine-containing acrylate copolymer and application as resins on dyed polyester microfiber fabric, J. Appl. Polym. Sci. 108 (3) (2008) 1778-1782. [7] K. Xie, J. Yu, D. Jiang, Shade darkening effect of polyorganosiloxane modified with amino and hydroxyl groups on dyed microfiber polyester fabric, J. Appl. Polym. Sci. 106 (2) (2007) 1256-1262. [8] H. Park, I. Yang, J. Wu, M. Kim, H. Hahm, S. Kim, Synthesis of silicone-acrylic resins and their applications to superweatherable coatings, J. Appl. Polym. Sci. 81 (7) (2001) 1614-1623. [9] D. Zhiping, Q. Jieqiong, W. Wanxu, Z. Yanyan, W. Guoyong, Synthesis, surface activities, and aggregation behaviors of butynediol-ethoxylate modified polysiloxanes, J. Phys. Chem. B 119 (3) (2015) 14180-14187. [10] H. Maciejewski, A. Wawrzynczak, M. Dutkiewicz, Silicone waxes-synthesis via hydrosilylation in homo-and het-erogeneous systems, J. Mol. Catal. A-Chem. 257 (1) (2006) 141-148. [11] F.X. Perrin, T.B.V. Nguyen, A. Margaillan, Linear and branched alkyl substituted octakis (dimethylsiloxy) octasilsesquioxanes: WAXS and thermal properties, Eur. Polym. J. 47 (7) (2011) 1370-1382. [12] E. Louis, I. Jussofie, F.E. Kuhn, Karstedt catalystcatalyzed stepgrowth co-polyaddition of 1,9-decadiene and 1,1,3,3-tetramethyl-disiloxane, J. Organomet Chem. 691 (9) (2006) 2031-2036. [13] H. Akverts, S. Kussi, W. Grape, Lubricating oil preparations, U.S. Pat., 4652386 (1987). [14] Q.J. Quaal, E.D. Groenh, R.J. Kelly, Metal working lubricant, U.S. Pat., 3756052 (1973). [15] C.C. Wang, L. Ekstrom, Video disc lubricants, U.S. Pat., 4342659 (1982). [16] S.T. Orszulik, Chemistry and Technology of Lubricants 3rd edn (eds. Orszulik, S.T. Fox, M.F.) (Dordrecht, Springer, New York, NY, USA, 2010). [17] Q.A. Syed, A comprehensive review of lubricant chemistry, technology, selection, and design (eds. Syed Q. A. Rizvi) (ASTM, International, 2009). [18] L.R. Rudnick, Synthetic Lubricants And High- Performance Functional Fluids, Revised And Expanded 2nd edn (eds. Rudnick, L.R. Shubkin, R. L.) (Ebrary, Inc., New York, NY, USA, 1999). [19] M. Torbacke, Lubricants: Introduction to Properties and Performance (eds. Torbacke, M. Kassfeldt, E. Rudolphi, A.K.) (West Sussex, Wiley, Sweden, Europe, 2014). [20] G.E. Legrow, Pristine alkylsiloxanes and method for their preparation, E.P. Pat., 0641799 (1995). [21] D. Edgar, J. Brown, N.Y. Schenectadey, Alkylpolysiloxane fluids, U.S. Pat., 3418353 (1968). [22] L. Larry N., On the mechanism of metal colloid catalyzed hydrosilylation: proposed explanations for electronic effects and oxygen cocatalysis, J. Am. Chem. Soc. 112 (16) (1990) 5998-6002. [23] C. Liujun, L. Qiongqiong, Z. Anqiang, Y. Lin, L. Yaling, Synthesis and Characterization of Carboxyl Terminated Polydimethylsiloxanes, J. Macromol. Sci. A 51 (1) (2014) 16-26. [24] H. Aiqin, Y. Jibin, S. Yaqi, Preparation and surface properties of the polysiloxane material modified with fluorocarbon side chains, Eur. Polym. J. 44 (6) (2008) 1696-1700.

3. 毕业设计（论文）进程安排

进程安排：1、3月份查阅文献，了解实验背景，设 计自己的实验方案。

2、4-5月份，做实验，整理数据，做好表征，撰写论文。