1. 毕业设计（论文）的内容和要求

内容： （1）创制硅酸锆-磺酸双改性介孔氧化硅催化剂；（2）表征催化剂微观结构；（3）探究双改性介孔氧化硅的催化性能及结构-性能关系。

要求：（1）具备开展文献检索、阅读和信息综合分析的能力。

（2）能够运用化学化工基础理论解决工艺研究和过程优化问题。

2. 参考文献

1. J. Machado, J.E. Castanheiro, I. Matos, A.M. Ramos, J. Vital, I.M. Fonseca, SBA-15 with sulfonic acid groups as a Green Catalyst for the acetoxylation of α-pinene, Microporous Mesoporous Materials, 163 (2012) 237-242. 2. X. Chen, J. Feng, Z. Fei, W. Sun, J. Tang, P. He, M. Cui, X. Qiao, Synthesis of tert-butyl acetate via eco-friendly additive reaction over mesoprous silica catalysts with balanced Br#246;nsted and Lewis acid sites, Journal of Porous Materials, 23 (2016) 255-262. 3. Dongyuan Zhao, #8225;, Qisheng Huo, #8225;, Jianglin Feng, B.F.C. And, #8225;, #167;, G.D.S. #8225;, #8224;,, Nonionic Triblock and Star Diblock Copolymer and Oligomeric Surfactant Syntheses of Highly Ordered, Hydrothermally Stable, Mesoporous Silica Structures, Journal of the American Chemical Society, 136 (1998) 6024-6036. 4. F. Kleitz, S.H. Choi, R. Ryoo, Cubic Ia3d large mesoporous silica: synthesis and replication to platinum nanowires, carbon nanorods and carbon nanotubes, Chemical Communications, 9 (2003) 2136-2137. 5. S.S. Reddy, B.D. Raju, V.S. Kumar, A.H. Padmasri, S. Narayanan, K.S.R. Rao, Sulfonic acid functionalized mesoporous SBA-15 for selective synthesis of 4-phenyl-1,3-dioxane, Catalysis Communications, 8 (2007) 261-266. 6. W. Li, S.J. Huang, S.B. Liu, M.O. Coppens, Influence of the Al source and synthesis of ordered Al-SBA-15 hexagonal particles with nanostairs and terraces, Langmuir the Acs Journal of Surfaces Colloids, 21 (2005) 2078-2085.

3. 毕业设计（论文）进程安排

2018.3.1--4.1 通过文献检索，阅读大量相关文献，并完成一篇英文文献的翻译；充分了解实验所需的药品和仪器，为实验做准备；正确认识自己的课题，完成开题报告。

4.1--4.15 根据实验安排进行实验，制备催化剂。

4.15-5.1 对实验结果及时分析、总结，不断调整实验方案；根据实验结果，完成论文中期报告。