1. 毕业设计（论文）的内容和要求

查阅相关文献与专业书籍了解目前水滑石制备方面研究的现状，了解该材料相关背景，了解其在苯酚羟基化反应催化中的应用，已有成果以及存在的问题，对论文的研究方向有较深入的认识。

本课题研究使用水热法制备铜镁铝水滑石材料及将其应用于苯酚羟基化反应中，并对水滑石材料的酸碱性对探针反应的影响进行探究。

本课题的研究手段： 1.查阅文献，了解课题相关背景，实验方法等； 2.考察催化剂结构；通过红外，xrd，sem 等手段表征与测定催化剂的机构和形貌。

2. 参考文献

1. Ikurumi, S.; Okada, S.; Nakatsuka, K.; Kamegawa, T.; Mori, K.; Yamashita, H., Enhanced Activity and Selectivity in the One-Pot Hydroxylation of Phenol by Pd/SiO2@Fe-Containing Mesoporous Silica Core#8211;Shell Catalyst. Journal of Physical Chemistry C 2015, 118 (1), 575#8211;581. 2. Li, S.; Li, G.; Li, G.; Wu, G.; Hu, C., Microporous carbon molecular sieve as a novel catalyst for the hydroxylation of phenol. Microporous Mesoporous Materials 2011, 143 (1), 22-29. 3. Xu, Y.; Liu, J.; Ma, G.; Wang, J.; Lin, J.; Wang, H.; Zhang, C.; Ding, M., Effect of iron loading on acidity and performance of Fe/HZSM-5 catalyst for direct synthesis of aromatics from syngas. Fuel 2018, 228, 1-9. 4. He, Z.; Wu, J.; Gao, B.; He, H., Hydrothermal synthesis and characterization of aluminum-free Mn-Icirc;sup2; zeolite: a catalyst for phenol hydroxylation. Acs Appl Mater Interfaces 2015, 7 (4), 2424-2432. 5. Mitnik, Y. V.; Oludipe, D. O.; Litvintsev, I. Y.; Sapunov, V. N., Catalytic oxidation of monosubstituted phenols by hydrogen peroxide. Reaction Kinetics Catalysis Letters 1991, 43 (2), 321-328. 6. Wang, L.; Kong, A.; Chen, B.; Ding, H.; Shan, Y.; He, M., Direct synthesis, characterization of Cu-SBA-15 and its high catalytic activity in hydroxylation of phenol by H 2 O 2. Journal of Molecular Catalysis A Chemical 2005, 230 (1), 143-150. 7. Pamin, K.; Po#322;towicz, J.; Prończuk, M.; Bas#261;g, S.; Maciejewska, J.; Kry#347;ciak-Czerwenka, J.; Tokarz-Sobieraj, R., Hydroxylation of phenol by hydrogen peroxide catalyzed by heteropoly compounds in presence of glycerol as green solvent. Catalysis Today 2015, 257, 80-85. 8. Changming, L.; Min, W.; Evans, D. G.; Xue, D., Layered double hydroxide-based nanomaterials as highly efficient catalysts and adsorbents. Small 2015, 10 (22), 4469-4486. 9. Taei, M.; Havakeshian, E.; Abedi, F.; Movahedi, M., The effect of Cu Mg Fe layered double hydroxide on the electrocatalytic activity of gold nanoparticles towards ethanol electrooxidation. International Journal of Hydrogen Energy 2016, 41 (31), 13575-13582.

3. 毕业设计（论文）进程安排

3月中旬完成开题报告；3月中旬-4月底完成实验内容及开始论文的撰写；5月上交论文初稿